Structures by: Yamaguchi K.
Total: 457
C18NMeCarbacage
C67H117NSi2
CrystEngComm (2019) 21, 26 3910
a=34.673(6)Å b=12.090(2)Å c=17.728(3)Å
α=90° β=119.214(2)° γ=90°
TMS2MeCarba
C19H27NSi2
CrystEngComm (2019) 21, 26 3910
a=15.104(7)Å b=6.317(4)Å c=20.8662(10)Å
α=90° β=96.345(11)° γ=90°
C180H112B4D84N4O34S14
C180H112B4D84N4O34S14
Organic letters (2015) 17, 9 2154-2157
a=16.670(3)Å b=17.440(4)Å c=19.659(4)Å
α=81.21(3)° β=74.06(3)° γ=62.19(3)°
C117H171B4N4O20
C117H171B4N4O20
Organic letters (2015) 17, 9 2154-2157
a=42.193(8)Å b=8.3560(17)Å c=15.630(3)Å
α=90° β=90.76(3)° γ=90°
C186H168B4N14O31
C186H168B4N14O31
Organic letters (2015) 17, 9 2154-2157
a=16.134(3)Å b=16.609(3)Å c=16.766(3)Å
α=85.82(3)° β=65.15(3)° γ=75.26(3)°
C50H44F24N4P4
C50H44F24N4P4
Organic letters (2015) 17, 9 2154-2157
a=13.488(3)Å b=14.281(3)Å c=14.287(3)Å
α=90° β=108.36(3)° γ=90°
C152.5H199B4N7O23
C152.5H199B4N7O23
Organic letters (2015) 17, 9 2154-2157
a=11.705(2)Å b=28.512(6)Å c=22.406(5)Å
α=90° β=98.94(3)° γ=90°
C14H29NO2Si
C14H29NO2Si
Organic letters (2016) 18, 7 1598-1601
a=7.852(3)Å b=8.477(4)Å c=14.445(6)Å
α=89.890(4)° β=75.960(4)° γ=65.051(4)°
C60H56N4O4
C60H56N4O4
Organic letters (2017) 19, 7 1508-1511
a=16.5759(6)Å b=13.1086(5)Å c=12.2124(5)Å
α=90° β=108.101(2)° γ=90°
C114.47H115.78B3N12.82O14.82
C114.47H115.78B3N12.82O14.82
Macromolecules (2017) 50, 20 8028
a=23.269(5)Å b=18.286(4)Å c=33.209(7)Å
α=90° β=92.92(3)° γ=90°
C24H28Cl3NO6PdS
C24H28Cl3NO6PdS
Chemical Science (2013) 4, 9 3753
a=9.3736(10)Å b=15.1780(11)Å c=10.1053(9)Å
α=90.00° β=107.302(4)° γ=90.00°
C43H31Cl6N2
C43H31Cl6N2
Organic letters (2014) 16, 17 4622
a=22.782(3)Å b=22.782(3)Å c=7.3730(15)Å
α=90.00° β=90.00° γ=90.00°
C50H42N4
C50H42N4
Organic letters (2014) 16, 17 4622
a=23.0796(14)Å b=23.0796(14)Å c=7.0154(6)Å
α=90.00° β=90.00° γ=90.00°
C102H70B4O20
C102H70B4O20
Organic letters (2015) 17, 10 2466-2469
a=30.624(13)Å b=56.38(2)Å c=22.177(9)Å
α=90° β=93.399(11)° γ=90°
C18cageNp
C64H114Si2
Organic letters (2013) 15, 19 5092-5095
a=14.5354(18)Å b=14.7161(18)Å c=16.738(2)Å
α=66.601(2)° β=82.719(2)° γ=68.828(2)°
C14satNpcage
C52H90Si2
Organic letters (2013) 15, 19 5092-5095
a=13.327(3)Å b=17.391(4)Å c=23.422(5)Å
α=93.875(3)° β=102.751(2)° γ=110.568(2)°
C16satNpcage
2(C58H102Si2),1.5(C4H8O)
Organic letters (2013) 15, 19 5092-5095
a=14.1947(12)Å b=15.1832(13)Å c=28.719(2)Å
α=85.1370(10)° β=80.2820(10)° γ=75.0800(10)°
C64H31Cl3O12
C64H31Cl3O12
Organic Letters (2013) 15, 9 2164
a=10.7990(2)Å b=17.2424(3)Å c=13.5434(2)Å
α=90.00° β=104.4400(10)° γ=90.00°
C45H27O8
C45H27O8
Organic Letters (2013) 15, 9 2164
a=14.714(3)Å b=22.636(4)Å c=9.8621(18)Å
α=90.00° β=90.00° γ=90.00°
C87H78O12,2(C60)
C87H78O12,2(C60)
Organic Letters (2013) 15, 9 2164
a=22.459(3)Å b=22.459(3)Å c=25.656(5)Å
α=90.00° β=90.00° γ=90.00°
C213H24O12
C213H24O12
Organic Letters (2013) 15, 9 2164
a=23.187(3)Å b=23.187(3)Å c=26.056(5)Å
α=90.00° β=90.00° γ=90.00°
C28H29NOS
C28H29NOS
Chemical Science (2012) 3, 6 2165
a=9.357(7)Å b=13.439(9)Å c=18.660(13)Å
α=90.00° β=90.00° γ=90.00°
C20H20N2O4S2
C20H20N2O4S2
Organic letters (2003) 5, 21 3939-3942
a=8.475(1)Å b=8.475(1)Å c=27.185(1)Å
α=90° β=90° γ=90°
C22H24N2O4S2
C22H24N2O4S2
Organic letters (2003) 5, 21 3939-3942
a=11.994(3)Å b=11.904(3)Å c=15.388(3)Å
α=90° β=90° γ=90°
C26H42O5Si2
C26H42O5Si2
Organic letters (2008) 10, 9 1803-1805
a=14.0993(17)Å b=16.560(2)Å c=12.0918(15)Å
α=90.00° β=104.882(2)° γ=90.00°
C216H244F72N48O20P12Pd12
C216H244F72N48O20P12Pd12
Organic letters (2007) 9, 7 1379-1382
a=20.9886(18)Å b=22.092(3)Å c=22.856(6)Å
α=104.509(6)° β=104.619(6)° γ=94.833(6)°
C48H42F12N4O4S2Zn
C48H42F12N4O4S2Zn
Organic letters (2007) 9, 3 509-512
a=13.3076(6)Å b=13.3076(6)Å c=27.1044(15)Å
α=90.0000° β=90.0000° γ=90.0000°
C29H34Br2O5Si
C29H34Br2O5Si
Organic letters (2006) 8, 9 1889-1891
a=11.4155(16)Å b=20.035(3)Å c=25.895(4)Å
α=90.00° β=93.774(3)° γ=90.00°
6,13-Bis(methylthio)pentacene
C24H18S2
Organic letters (2006) 8, 11 2385-2388
a=5.1281(9)Å b=17.586(3)Å c=9.3323(16)Å
α=90.00° β=95.199(2)° γ=90.00°
C28H31BrO3Si
C28H31BrO3Si
Organic letters (2005) 7, 26 5913-5915
a=30.718(3)Å b=6.6546(6)Å c=26.833(3)Å
α=90.00° β=105.942(2)° γ=90.00°
[Rh(dtbpb)(nbd)]PF6
C29H48P2Rh1,F6P1,C4H8O
Organic letters (2006) 8, 26 6103-6106
a=11.1077(6)Å b=11.1077(6)Å c=24.942(3)Å
α=90.00° β=90.00° γ=120.00°
C16H17NO3
C16H17NO3
Organic letters (2007) 9, 26 5545-5547
a=8.9486(17)Å b=13.132(3)Å c=12.841(3)Å
α=90.00° β=109.123(3)° γ=90.00°
C14H13NO3
C14H13NO3
Organic letters (2007) 9, 26 5545-5547
a=6.34270(10)Å b=11.2959(2)Å c=16.3905(4)Å
α=90.00° β=90.00° γ=90.00°
C14H11NO3
C14H11NO3
Organic letters (2007) 9, 26 5545-5547
a=11.58(1)Å b=15.72(3)Å c=6.701(7)Å
α=90.0000° β=90.0000° γ=90.0000°
C258H579N17O156Si4Ti8W40
C258H579N17O156Si4Ti8W40
Inorganic Chemistry (2006) 45, 5 2347-2356
a=29.166Å b=38.497Å c=37.405Å
α=90° β=90° γ=90°
C100H212K8O128S2Si2Ti4W20
C100H212K8O128S2Si2Ti4W20
Inorganic Chemistry (2006) 45, 5 2347-2356
a=33.2107(3)Å b=35.4445(4)Å c=85.0187(8)Å
α=90.0000° β=90.0000° γ=90.0000°
C98H200K8O126Si2Ti4W20
C98H200K8O126Si2Ti4W20
Inorganic Chemistry (2006) 45, 5 2347-2356
a=45.4319(7)Å b=17.8884(4)Å c=15.8179(3)Å
α=90.0000° β=96.3280(8)° γ=90.0000°
C104N6O82P2Ti4W20
C104N6O82P2Ti4W20
Catal. Sci. Technol. (2015) 5, 10 4778
a=23.11120(10)Å b=15.27010(10)Å c=27.7104(2)Å
α=90.00° β=108.7383(4)° γ=90.00°
O80P2Ti4W20
O80P2Ti4W20
Catal. Sci. Technol. (2015) 5, 10 4778
a=20.570(4)Å b=34.716(7)Å c=54.711(11)Å
α=88.88(3)° β=85.12(3)° γ=79.80(3)°
C66H60Cl9N6O6P3
C66H60Cl9N6O6P3
Organic letters (2015) 17, 15 3650-3653
a=17.622(5)Å b=17.622(5)Å c=37.634(11)Å
α=90.00° β=90.00° γ=120.00°
C66H65N6O7P3
C66H65N6O7P3
Organic letters (2015) 17, 15 3650-3653
a=12.580(4)Å b=13.197(4)Å c=19.419(6)Å
α=80.816(5)° β=80.935(4)° γ=69.837(4)°
C67H63N8O6P3
C67H63N8O6P3
Organic letters (2015) 17, 15 3650-3653
a=13.731(3)Å b=14.962(3)Å c=15.117(3)Å
α=94.572(3)° β=91.240(3)° γ=101.538(3)°
C67H65N6O8P3
C67H65N6O8P3
Organic letters (2015) 17, 15 3650-3653
a=13.721(5)Å b=14.840(6)Å c=15.073(6)Å
α=94.518(5)° β=91.104(5)° γ=100.582(5)°
C63H57N6O9P3
C63H57N6O9P3
Organic letters (2015) 17, 15 3650-3653
a=13.914(3)Å b=13.914(3)Å c=28.339(7)Å
α=90.00° β=90.00° γ=120.00°
C65H63N6O7P3S
C65H63N6O7P3S
Organic letters (2015) 17, 15 3650-3653
a=13.123(2)Å b=13.188(2)Å c=19.257(3)Å
α=73.751(2)° β=79.260(2)° γ=66.588(2)°
C270H372B6N8O30
C270H372B6N8O30
Organic letters (2015) 17, 10 2466-2469
a=52.579(11)Å b=21.835(4)Å c=29.598(6)Å
α=90° β=117.54(3)° γ=90°
C64H68Cl4N4O10
C64H68Cl4N4O10
CrystEngComm (2020)
a=17.217(3)Å b=11.2747(18)Å c=16.415(3)Å
α=90° β=117.459(3)° γ=90°
C64H68Cl4N4O7
C64H68Cl4N4O7
CrystEngComm (2020)
a=17.1722(16)Å b=11.3008(10)Å c=16.1727(15)Å
α=90° β=117.160(2)° γ=90°
C60H54Cl4N4O4
C60H54Cl4N4O4
CrystEngComm (2020)
a=16.5240(14)Å b=13.9309(12)Å c=11.3445(9)Å
α=90° β=107.390(3)° γ=90°
C59H52Cl4N4O4
C59H52Cl4N4O4
CrystEngComm (2020)
a=13.6415(17)Å b=11.1851(14)Å c=32.017(4)Å
α=90° β=90° γ=90°
C54H48Cl8N4O4
C54H48Cl8N4O4
CrystEngComm (2020)
a=16.397(4)Å b=13.840(3)Å c=11.647(3)Å
α=90° β=108.793(3)° γ=90°
C54H46Cl10N4O4
C54H46Cl10N4O4
CrystEngComm (2020)
a=11.8817(5)Å b=13.9512(6)Å c=30.8666(13)Å
α=90° β=90° γ=90°
C96H80O28P4V10
C96H80O28P4V10
Green Chemistry (2020) 22, 12 3896-3905
a=12.2892(4)Å b=20.1324(4)Å c=18.9867(5)Å
α=90° β=102.411(3)° γ=90°
C64H58Cl6N4O12
C64H58Cl6N4O12
CrystEngComm (2020)
a=7.6112(5)Å b=11.9128(7)Å c=16.0046(10)Å
α=81.915(3)° β=81.796(3)° γ=80.150(3)°
C64H58Cl6N4O11
C64H58Cl6N4O11
CrystEngComm (2020)
a=7.6225(8)Å b=12.0460(13)Å c=15.9044(17)Å
α=81.746(5)° β=80.373(5)° γ=79.855(5)°
C64H58.01Cl5.97N4O12
C64H58.01Cl5.97N4O12
CrystEngComm (2020)
a=7.6781(5)Å b=12.0451(8)Å c=15.9522(11)Å
α=81.688(3)° β=81.540(3)° γ=79.019(3)°
C63H56Cl6N4O12
C63H56Cl6N4O12
CrystEngComm (2020)
a=7.6120(5)Å b=12.0404(7)Å c=15.8636(10)Å
α=81.859(2)° β=81.279(2)° γ=80.545(2)°
C210H270B6N6O24
C210H270B6N6O24
Organic & biomolecular chemistry (2020) 18, 19 3717-3723
a=42.922(9)Å b=30.652(6)Å c=19.133(4)Å
α=90° β=94.97(3)° γ=90°
C223.49H272.13B6N6.66O25.16
C223.49H272.13B6N6.66O25.16
Organic & biomolecular chemistry (2020) 18, 19 3717-3723
a=27.909(6)Å b=32.780(7)Å c=34.958(7)Å
α=105.11(3)° β=107.86(3)° γ=110.03(3)°
C45H39N3O3
C45H39N3O3
Organic & biomolecular chemistry (2020) 18, 2 230-236
a=9.47394(8)Å b=19.77494(10)Å c=19.02693(13)Å
α=90.0000° β=101.6839(8)° γ=90.0000°
C87H79N6O7
C87H79N6O7
Organic & biomolecular chemistry (2020) 18, 2 230-236
a=14.89204(7)Å b=17.25623(10)Å c=28.41877(13)Å
α=90.0000° β=98.1145(4)° γ=90.0000°
C33H25NO2
C33H25NO2
Organic & biomolecular chemistry (2010) 8, 9 2174-2179
a=13.05670(10)Å b=9.25440(10)Å c=19.7847(2)Å
α=90.00° β=100.23° γ=90.00°
C33H25NO2
C33H25NO2
Organic & biomolecular chemistry (2010) 8, 9 2174-2179
a=12.4729(12)Å b=13.3772(13)Å c=13.8882(13)Å
α=90.00° β=90.00° γ=90.00°
C33H25NO2
C33H25NO2
Organic & biomolecular chemistry (2010) 8, 9 2174-2179
a=9.4894(18)Å b=27.726(5)Å c=9.0631(17)Å
α=90.00° β=90.00° γ=90.00°
C50H82N30O31Pt
C50H82N30O31Pt
Organic & biomolecular chemistry (2005) 3, 11 2122-2125
a=23.6543(5)Å b=30.23670(10)Å c=31.2827(6)Å
α=90.00° β=90.00° γ=90.00°
C10H8N2O3
C10H8N2O3
Organic & biomolecular chemistry (2017) 15, 6 1381-1392
a=19.170(3)Å b=5.9569(10)Å c=7.7612(14)Å
α=90° β=90° γ=90°
C18H18ClNO6S2
C18H18ClNO6S2
Organic & biomolecular chemistry (2017) 15, 6 1381-1392
a=12.5262(12)Å b=9.5955(9)Å c=16.6342(15)Å
α=90° β=93.049(3)° γ=90°
C13H15BrClNO
C13H15BrClNO
Organic & biomolecular chemistry (2017) 15, 6 1381-1392
a=10.5871(9)Å b=17.4471(15)Å c=7.3732(6)Å
α=90° β=107.844(3)° γ=90°
C37H69N5O6Si4
C37H69N5O6Si4
Organic & biomolecular chemistry (2011) 9, 16 5633-5636
a=9.84534(19)Å b=13.7667(3)Å c=35.6430(7)Å
α=90.0000° β=90.0000° γ=90.0000°
MolGyro
C60H112Si2
Organic & biomolecular chemistry (2014) 12, 21 3354-3357
a=12.308(7)Å b=13.358(7)Å c=18.357(10)Å
α=76.993(7)° β=87.634(8)° γ=86.828(7)°
MolGyroIsomer
C60H112Si2
Organic & biomolecular chemistry (2014) 12, 21 3354-3357
a=14.530(3)Å b=18.768(3)Å c=21.753(4)Å
α=95.313(2)° β=90.751(3)° γ=92.942(2)°
C26H40O2S2Si2
C26H40O2S2Si2
Organic & biomolecular chemistry (2015) 13, 21 5964-5971
a=11.205(3)Å b=11.346(3)Å c=13.093(4)Å
α=108.312(3)° β=90.218(3)° γ=112.482(3)°
2,7-TMSpyrene
C22H26Si2
Organic & biomolecular chemistry (2015) 13, 42 10511-10516
a=6.3540(12)Å b=16.626(3)Å c=9.3688(17)Å
α=90.00° β=100.456(2)° γ=90.00°
C18Pycage
C70H116Si2
Organic & biomolecular chemistry (2015) 13, 42 10511-10516
a=12.173(3)Å b=17.375(4)Å c=18.275(4)Å
α=61.920(3)° β=71.547(3)° γ=87.263(3)°
C26H70Br2Mn2O2Si8
C26H70Br2Mn2O2Si8
Dalton transactions (Cambridge, England : 2003) (2020) 49, 48 17537-17541
a=9.482(4)Å b=10.595(4)Å c=13.023(5)Å
α=90.848(4)° β=107.188(5)° γ=96.065(5)°
C32H70MnN4Si4
C32H70MnN4Si4
Dalton transactions (Cambridge, England : 2003) (2020) 49, 48 17537-17541
a=10.0789(16)Å b=23.499(4)Å c=18.131(3)Å
α=90.0000° β=90.882(2)° γ=90.0000°
C40H96Mn2N4Si8
C40H96Mn2N4Si8
Dalton transactions (Cambridge, England : 2003) (2020) 49, 48 17537-17541
a=9.769(4)Å b=12.962(5)Å c=14.713(5)Å
α=97.083(5)° β=97.254(5)° γ=108.321(5)°
C34H88Mn2O4Si8
C34H88Mn2O4Si8
Dalton transactions (Cambridge, England : 2003) (2020) 49, 48 17537-17541
a=9.820(4)Å b=9.922(4)Å c=14.623(5)Å
α=97.082(5)° β=98.990(4)° γ=100.713(6)°
C124Cl12N7O73Si2Sn6W18
C124Cl12N7O73Si2Sn6W18
Chemical communications (Cambridge, England) (2016) 52, 70 10688-10691
a=18.75170(10)Å b=28.4384(3)Å c=21.5390(2)Å
α=90° β=115.1216(3)° γ=90°
C115N10O77Si2Sn6W18
C115N10O77Si2Sn6W18
Chemical communications (Cambridge, England) (2016) 52, 70 10688-10691
a=17.6999(2)Å b=18.7362(2)Å c=29.8744(4)Å
α=82.6590(10)° β=88.2780(10)° γ=74.2910(10)°
C10H10N2
C10H10N2
Chemical communications (Cambridge, England) (2018) 54, 15 1881-1884
a=8.9125(14)Å b=11.3351(18)Å c=13.323(2)Å
α=69.182(2)° β=74.864(2)° γ=87.348(2)°
C14H17F6N2OP
C14H17F6N2OP
Chemical communications (Cambridge, England) (2018) 54, 15 1881-1884
a=9.3512(9)Å b=14.2117(14)Å c=12.5086(12)Å
α=90° β=110.717(2)° γ=90°
C12H16BrF6N2P
C12H16BrF6N2P
Chemical communications (Cambridge, England) (2018) 54, 15 1881-1884
a=8.4310(7)Å b=10.6455(9)Å c=17.7568(14)Å
α=90° β=91.537(2)° γ=90°
C13H17F6N2P
C13H17F6N2P
Chemical communications (Cambridge, England) (2018) 54, 15 1881-1884
a=8.8739(5)Å b=12.9265(7)Å c=13.4682(7)Å
α=90° β=99.885(2)° γ=90°
C84Ag2CrMn4N7O70Si2W18
C84Ag2CrMn4N7O70Si2W18
Chem. Commun. (2017)
a=14.5907(2)Å b=14.8029(2)Å c=19.3294(3)Å
α=68.6210(10)° β=80.4000(10)° γ=66.5450(10)°
C132Cl8CrLu2Mn4N7O78Si2W18
C132Cl8CrLu2Mn4N7O78Si2W18
Chem. Commun. (2017)
a=19.3682(2)Å b=22.8418(3)Å c=26.9735(4)Å
α=87.3100(10)° β=78.6320(10)° γ=85.3220(10)°
C116Ag2CrLu2Mn4N14O78Si2W18
C116Ag2CrLu2Mn4N14O78Si2W18
Chem. Commun. (2017)
a=17.4607(3)Å b=18.5296(6)Å c=19.3013(3)Å
α=61.2950(10)° β=63.2520(10)° γ=82.4150(10)°
C120Cl8CrMn4N7O70Si2W18
C120Cl8CrMn4N7O70Si2W18
Chem. Commun. (2017)
a=14.32460(10)Å b=20.0905(2)Å c=34.1760(4)Å
α=102.4516(6)° β=96.5392(6)° γ=93.5466(4)°
C41.28H29.31EuN0.76O8P
C41.28H29.31EuN0.76O8P
New J. Chem. (2017)
a=36.205(7)Å b=15.379(3)Å c=29.692(6)Å
α=90° β=90° γ=90°
C128N15O69Si2W20Zn
C128N15O69Si2W20Zn
New J. Chem. (2017)
a=18.23880(10)Å b=51.6192(4)Å c=20.9479(2)Å
α=90° β=102.4143(3)° γ=90°
C124Cl12N7O70Si2VW18
C124Cl12N7O70Si2VW18
Journal of Materials Chemistry C (2019) 7, 41 12918
a=14.6894(4)Å b=18.7501(3)Å c=19.1270(5)Å
α=107.0720(10)° β=91.9510(10)° γ=97.900(2)°
C116Mn4N11O78Si2VW18
C116Mn4N11O78Si2VW18
Journal of Materials Chemistry C (2019) 7, 41 12918
a=28.5552(2)Å b=22.3557(2)Å c=29.6380(2)Å
α=90° β=105.0709(2)° γ=90°
C38H39Cl2N4O6
C38H39Cl2N4O6
CrystEngComm (2018) 20, 38 5667
a=10.7680(5)Å b=12.2601(6)Å c=13.3043(6)Å
α=97.054(2)° β=101.999(2)° γ=98.839(2)°
C34H34Cl2N4O6
C34H34Cl2N4O6
CrystEngComm (2018) 20, 38 5667
a=23.5127(11)Å b=7.1104(3)Å c=19.6874(9)Å
α=90° β=108.636(2)° γ=90°
C34H34Cl2N4O6
C34H34Cl2N4O6
CrystEngComm (2019) 21, 10 1548
a=19.6020(17)Å b=10.4596(9)Å c=15.8952(14)Å
α=90° β=107.358(2)° γ=90°
C39H43Cl2N4O6
C39H43Cl2N4O6
CrystEngComm (2019) 21, 10 1548
a=10.0070(5)Å b=13.2653(7)Å c=15.0577(8)Å
α=80.234(2)° β=71.193(2)° γ=70.137(2)°
C37.5H40Cl2N4O6
C37.5H40Cl2N4O6
CrystEngComm (2019) 21, 10 1548
a=9.9312(5)Å b=13.0381(7)Å c=14.9669(8)Å
α=78.504(2)° β=71.545(2)° γ=71.592(2)°
C38H42Cl2N4O6
C38H42Cl2N4O6
CrystEngComm (2019) 21, 10 1548
a=9.9249(9)Å b=13.0873(12)Å c=15.1023(14)Å
α=78.486(3)° β=71.671(3)° γ=71.466(3)°
C37.5H41Cl2N4O6
C37.5H41Cl2N4O6
CrystEngComm (2019) 21, 10 1548
a=9.9369(5)Å b=13.0256(7)Å c=14.9773(8)Å
α=78.670(3)° β=71.719(3)° γ=71.595(3)°